PEFTEC 2019 – Re-engineering Calibration for Process Spectrometers

Re-engineering Calibration for Process Spectrometers – This is a report of a multi-company, multi-industry, hydrocarbon processing consortium, established six years ago, to re-evaluate how the calibration process for analyzers could be managed more efficiently. The first focus was optical spectroscopy, an increasingly important source of process chemistry knowledge due to its advantage of speed, sensitivity, and simple safety requirements. As one of very few analyzer technologies that can measure chemistry, spectroscopy has become a workhorse in the chemical, petrochemical, and petroleum industries. But, even as the number of optical systems is continuing to increase, companies have been decreasing the number of employees who are tasked with their management. As a result, a paradigm shift is required for industry to adapt to a higher workload combined with changes in the fitness level and longevity of the technicians responsible for installation, calibration, and maintenance. What if we could put a spectroscopy system in place and have it handle the application and communicate results as soon as it is turned on? Then, if performance does not match legacy standards, the system dials itself in or calls for help. The systematic approach discussed is not constrained by the brand of hardware or by the software vendor and, as such, the approach can be used to manage any new or any in-place system. Presented by Brian Rohrback, Infometrix, Inc.

ISA AD 2019 Short course – Multivariate Analysis for Inferentials and Analyzers

Multivariate Analysis for Inferentials and Analyzers This course examines a series of algorithmic approaches with the goal of streamlining multivariate model construction to make the analyzers significantly more robust when put into routine practice. This class will benefit those who want to better understand the tools available to build qualitative and quantitative inferentials for their process. It will also benefit technicians who perform both routine and irregular maintenance of chromatographic and spectroscopic instruments in both process and laboratory settings. Managing pressure, temperature, flow and level as an ensemble rather than as independent measurements to track will be highlighted. Attention will also be aimed at optical spectrometers, in particular near infrared and Raman. Chromatographic applications will be discussed with the purpose of simplifying maintenance. These topics are designed to cover the best practices of multivariate technology and will prepare participants for tackling a vast array of problems. This course is useful for any chemist or engineer who is concerned about optimizing their analytical methods to get the most out of their process operations. This course will be presented by Brian Rohrback, president of Infometrix, Inc.

Gulf Coast Conference, October 16-17, 2018

Gulf Coast Conference
Oct 16-17, 2018
Galveston, TX

 

Infometrix will be attending the 2018 Gulf Coast Conference in October. See abstracts below for the 2018 presentations at the GCC conference by Infometrix. Join us or contact us for more information.

Abstract # 169 – Paper
10/16/2018 – 1:20 PM – 1:40 PM – Tulip Room

Optimizing Gas Chromatography
Brian Rohrback – Infometrix

The heartbeat of the process environment is in the data we collect, but we are not always efficient in translating our data streams into actionable information. The richest source of hydrocarbon process information comes from spectrometers and chromatographs and, for many applications, gas chromatography is the cheapest, most adaptable, and most reliable technology available.  We can use tech borrowed from other fields to provide more consistent and objective GC results, automate translation of the raw traces into real-time information streams, and create databases that can be used across plant sites or even across industries.

 

Abstract # 145 – Paper
10/16/2018 – 10:45 AM – 11:05 AM – Tulip Room

Automating Spectroscopy Calibrations
Brian Rohrback – Infometrix, Inc.

A consortium of companies has undertaken a project to reduce the effort devoted to producing, maintaining, and stabilizing optical spectroscopy performance in routine quality assessment. Over a five-year period, the group has examined an unprecedented historical collection of spectra from multiple spectrometers spanning 1-5 years from sixteen oil refineries, with the goal of developing and maintaining stable models for long-term deployment. Even though the data are tied to petroleum work, the lessons learned are true for all applications. The technologies utilized follow a pattern of best practices, including the use of Robust outlier diagnostics, local and hierarchical modeling, and model augmentation. The effort has resulted in significant progress towards automation of model creation, stability, and maintenance in an industrial process. Additionally, we will share a comparison of prediction capabilities of different spectroscopy technologies and form-factors that can lead to a significant reduction in deployment and maintenance cost.

 

ISA-AD Advanced Course: Multivariate Analysis for Inferentials and Analyzers

ISA AD 2018 Advanced Analyzer CourseRegister to learn chemometrics best practices to make analyzers significantly more robust when put into routine practice. The course covers the best practices of multivariate technology and will prepare you to tackle a vast array of problems. This course is useful for any chemist or engineer who is concerned about optimizing their analytical methods to get the most out of their process operations. Click on the banner image to the left for more information and how to register.